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Nitroxides (TEMPO), 14–17 nitronyl nitroxides 18–20 and tripheylmethyl 21–23 radicals have been successfully employed to prepare such paramagnetic hybrid materials. More recently, alkyne terminated derivatives have started to play a role. ![]() Usually thiols and disulfides are chosen to covalently modify gold surfaces, including gold nanoparticles, with organic radicals by adsorption from solution. However, the radical functionalization of a substrate is eased by choosing a specific chemical group that has a high chemical affinity for the selected substrate. 9 Our work indicated the need for identifying strategies in order to attach the radical to the surface preserving its magnetic moment at the interface by using different methods ranging from evaporation to preparation in a wet environment. 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